Ball milling The mechanical milling was carried out with a high energy ball mill Spex 8000 TCP samples were milled for different periods 0 5 10 and 15 h to obtain TCP TCP5 TCP10 and TCP15 samples respectively The tribasic calcium phosphate powder was placed into a
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Appropriate amount of deionized water and then put them into a ball mill ball milling finally the ballmilled powder was placed in a muffle furnace and heated to 800 176 c at 5 176 c min constant temperature for 24 hours after the temperature was cooled to room
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